Reaction kettle feeding work
The feeding work of the reactor has the following points: * * 1. Solid Material Charging ** 1. * * Material Pretreatment ** - For block-like solid materials, they needed to be processed into small pieces before being thrown into the reaction kettle. This would help the materials mix better with the liquid in the reaction kettle and improve the reaction efficiency. 2. * * Stirrer related operations ** - Before starting the stirring, first use your hand to rotate the stirring device to ensure that it does not get stuck or collide with easily damaged parts such as the thermometer tube. Then, press the electric switch to activate it. When the agitators can operate normally, then officially start the agitation operation. It is strictly forbidden to start it by force, so as to prevent solid materials from being stuck or colliding with the thermometer tube, causing equipment damage or test failure. 3. * * To prevent damage to the pot wall and falling into hard objects ** - When adding solid materials, be careful to avoid damaging the pot wall. If there is a dangerous medium in the reaction kettle, it is strictly forbidden for metal or hard objects to fall into the pot. * * 2. Liquid Material Charging ** 1. * * Vacuum pumping condition ** - If the liquid material is put in by vacuum pumping, the vacuum valve should be delayed to prevent flushing. Before opening the vacuum valve, he had to first ensure that the pressure in the reaction kettle was stable, and then gradually open the valve to allow the liquid material to slowly enter the reaction kettle. * * 3. Inspection before feeding ** 1. * * Material Inspection ** - Before feeding the materials into the reactor, the materials must be subjected to "self-inspection, re-inspection, and special inspection". Only when the "three inspections" are consistent can the materials be fed into the reactor. * * IV. Other precautions during feeding ** 1. * * According to the process operation procedure ** - In the process of adding materials, the time, speed, type, number, temperature rise, temperature drop, and heat preservation must be carried out in accordance with the process operation procedures to ensure the accuracy and reliability of the experimental results. 2. * * Surveillance during closed reaction ** - During the closed reaction, one needed to constantly observe the pressure, temperature, and other parameters inside and outside the kettle. If abnormal situations are discovered, measures should be taken in time to prevent safety accidents. For example, if the pressure was too high or the temperature was too high, it might cause the reactor to rupture or cause other safety accidents. 3. * * Equipment Operation Check ** - After the power is connected, the motor should drive the stirring operation, and check whether there is any state change phenomenon, sound, etc. in the transmission parts such as the decelerator and stirring to ensure the normal operation of the equipment, and find and deal with potential problems in time. If any abnormal phenomenon or sound is found, it should be immediately shut down for inspection to prevent equipment damage or affect the experiment results. 4. * * Personnel and product safety ** - Pay attention to personal safety and product safety at all times when feeding materials into the kettle. 5. * * Record and clean up ** - After feeding the materials, they had to re-check and sign the "Material List" for confirmation, and then clean up the garbage on the spot in time. Read more exciting novels for free
Industrial reaction kettle
Industrial reactors can be divided into three types according to their structural forms: open (open), closed (closed), and semi-open and semi-closed; according to the heat transfer method, they can be divided into external circulation type, internal circulation type, and direct flow type; according to the heating medium, they can be divided into water-cooled, oil-cooled, and air-cooled jacket heating types. The materials of the reactor were carbon steel, stainless steel, and so on. The process includes putting the materials into the stirring tank for heating and stirring. After reaching the set temperature, close the feeding valve and then open the discharge valve. The materials transfer heat to the cooling tank through the heat exchange and then enter the splitter. The magnetic stirring rod in the splitter is used to clarify the liquid phase. After the liquid phase is filtered, it enters the measuring tank and then is recycled through the return pipe. The concentrated solid particles are processed. When cleaning, open the discharge valve and wash with a high-pressure pump. After checking that there is no problem, it can be put into use. If you need more information about industrial reactors, you can further consult the relevant information. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Reaction Kettle, Enamel Kettle, Stainless Steel Kettle, Storage Tank
The reaction kettle was a type of pressure vessel used to complete the processes of sulfidification, nitration, dehydration, dehydration, condensation, and so on. Commonly seen were porcelain reaction kettles and stainless steel reaction kettles. The porcelain reactor was made of carbon steel. A layer of porcelain was burned on the surface of the contact material. The anti-corrosion ability of the porcelain layer was used to isolate the contact between the material and the carbon steel to protect the reactor body from corrosion. The temperature of the material could not exceed 200 degrees Celsius. If the temperature was too high, it would cause the glaze layer to melt. It was an open structure. The upper head and the kettle body were connected by a flange-like connection and filled with an anti-corrosion sealing mat. The pressure that could be maintained in the kettle did not exceed 4 kg. It is suitable for corrosive materials. The stainless steel reactor was made of stainless steel. According to the requirements of the material, it could be equipped with heating, cooling, high pressure, vacuum and other functions. The material temperature could reach 400 degrees Celsius, and the kettle could maintain a pressure of tens of kilograms or even hundreds of kilograms, but its corrosion resistance was worse than that of the porcelain reactor. However, the information provided by the storage tank did not include detailed information about the comparison of the reactor functions with the porcelain kettle and the stainless steel kettle. It was impossible to give detailed information under the same logic as the former two. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Dongyang plastic reaction kettle
Based on the available information, Dongyang City Yonggu chemical equipment factory has been committed to the development of tube reactor projects for six years. It is the first enterprise in the industry to adopt the cooling technology of the pp-type graphene tube. The cooling effect is doubled compared to the coil type. However, there is no more special information about Dongyang's pp-type plastic reactor, so it is impossible to answer in detail. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Zhongwei heating reaction kettle
Prerex Magnetic Reaction Kettle
Premex was a brand with 40 years of experience in the production of reactors. Its reactor volumes ranged from 100ml to 100L, pressures ranged from 6 bar to 700 bar, and the highest temperature could reach 350 ° C. It was made of various materials, including stainless steel, acid resistance, and special alloys. In addition to conventional products, we can also develop, design, and produce a variety of magnetic stirring heads and magnetic stirring drives. In terms of control and adjustment of high-pressure reactors, it can meet the needs of process control from simple controllers to complex software control, so as to meet the needs of complete installation or customer's individual requirements. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Disperse dye reaction kettle
A reaction kettle used for producing heat-resistant disperse dye includes a reaction kettle shell, the side wall of the reaction kettle shell is provided with a cylindrical temperature control cavity, the upper end of the temperature control cavity is communicated with a liquid injection pipe, the lower end of the temperature control cavity is communicated with a liquid discharge pipe, and the liquid injection pipe and the liquid discharge pipe are fixedly connected with the reaction kettle shell. The temperature control cavity is provided with a number of evenly distributed control devices, which include two protruding pieces, an intercepting cylinder, a sealing block and a gear. The protruding piece is fixed on the side wall of the inner cavity of the shell of the reaction kettle; the intercepting cylinder and the sealing block are arranged in the inner cavity of the temperature control chamber; the lower end of the sealing block extends into the intercepting cylinder; the upper end of the sealing block is connected with a gear; the gear is positioned in a cuboid-shaped groove arranged on the side wall of the temperature control chamber; one end of the gear is in transmission connection with a transmission rod; one end of the transmission rod is fixedly connected with a handle; the other end of the transmission rod extends into the side wall of the reaction kettle; and the handle is positioned outside the reaction kettle. The intercepting cylinder is cylindrical and is provided with a number of uniformly arranged diffusing pipe cavities; the lower end of the sealing block runs through the diffusing pipe cavities; the sealing block is cylindrical and is uniformly provided with prism-shaped protruding teeth on the outer wall; and the protruding teeth of the sealing block are engaged and connected with the gear. The intercepting cylinder is provided with a cylindrical groove and is communicated with the diffusing pipe cavity; the diffusing pipe cavity runs through the cylindrical groove; the lower end of the cylinder of the sealing block extends into the cylindrical groove of the intercepting cylinder; and the outer wall of the sealing block and the inner wall of the cylindrical groove of the intercepting cylinder are both in threaded connection. In addition, the dye reaction kettle and the dye dispersing kettle are used in the paint, coating, oil, chemical, rubber, pesticide, dye, medicine, food and other industries to complete the operation of stirring, dissolving and dispersing, and color matching. It has the functions of low-speed strong stirring and high-speed dispersing. It has good adaptability to medium and high-viscous and thixophic materials. Stirring and dispersing can be carried out at the same time. The stirring forms are generally anchor type, paddle type, turbine type, propeller type or frame type. When the stirring device is relatively large in height and diameter, multi-layer stirring blades can be used, and it can also be selected according to the user's requirements. Moreover, a jacket can be set outside the kettle wall, or a heat exchange surface can be set inside the vessel, and heat exchange can also be carried out through external circulation. The low-speed stirrers in the multi-functional reactor are usually of the frame type, paddle type, and frame anchor type. The stirring speed range is 0 - 130r/min. It is mainly used for the initial stirring of materials to prepare for the subsequent process of dispersing and vaporizing. The outer edge of the multi-functional stirring can be equipped with scraping plates to achieve uniform stirring without dead ends. The dispersing disc of the high-speed dispersing device is sawtooth-shaped. When rotating at a high speed, it forms a strong turbulent zone. The pulp layers with different flow rates diffuse each other to achieve the purpose of rapid dispersion. The speed of the dispersing shaft can be adjusted from 0 to 1200r/min. Butterfly stirring blades can also be installed, which is conducive to the mutual dissolving of viscous materials during the stirring process. Through the cooperation of the fast-moving rotating rotating motor and the precise motor, the kneading machine head can produce powerful hydraulic cutting, squeezing, cutting and other functions to achieve the purpose of uniform kneading. In actual production applications, the electrical control box can control the low-speed stirring device, high-speed dispersing device, and kneading machine separately or in combination to meet the requirements of different production processes and ensure that the product performance meets the standards. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Reaction kettle reconstruction construction plan
The following are some common construction plans for the reactor: ** I. Electromagnetic heating modification plan for the reactor ** 1. ** Power calculation and selection ** - First of all, the known conditions must be clear, such as the material, size (diameter, height, thickness, etc.), weight, effective volume, material weight, material mixing heat, heating temperature requirements, time requirements, etc. - According to the heat calculation formula,[Q = cm/Delta t+km](where [c] is the specific heat capacity,[m] is the mass, and [Delta t] is the temperature difference), the specific heat capacity [J/(KG* ° C)], the temperature difference [° C], and the mass [KG] are substituted into the formula and divided by the time [S] to obtain the power [W]. - For example, the known atmospheric pressure reactor, material 304, the external dimensions of the kettle body are 2 meters in diameter * 3 meters in height (8mm in thickness), the weight is about 1000kg, the effective volume is 7 m3, the material weight is 7 tons, the reaction material is a certain liquid material mixed specific heat according to the requirements of 4200J/kg* ° C, and it is required to be heated from 20 ° C to 280 ° C within 3 hours. After calculating the theoretical power, it is necessary to consider the loss (generally increase the loss by 20%) to determine the actual matching power. For example, the theoretical power of the above example is 708KW, and the actual matching is 708KW *1.2 = 850KW. Seven sets of 120KW electromagnetic heater can be used for parallel heating. 2. ** Steps to design the plan ** - Understand the original structure and working principle of the reactor, including the size, shape, material, working temperature and other parameters of the reactor. Then, according to the actual situation and needs of the reactor, the electromagnetic heating scheme was designed. ** II. Upgrade plan for the support and foam plug at the bottom of the reactor ** 1. ** Selection of Upgrade Materials ** - High-quality steel was used to ensure the bearing capacity and corrosion resistance of the lower support and foam plug. 2. ** Pre-construction preparation ** - The original lower support and foam plug were first cleaned, and then disassembled to facilitate the installation of new materials. 3. ** installation process ** - After determining the size of the new material, he drilled a hole and installed it gently. Then, he adjusted the reaction kettle to ensure that the new support and foam plug were stable. ** 3. Cleaning and replacement of paint containers ** 1. ** Clean paint container ** - Clean up the old paint container, use professional equipment to heat and spray it with high pressure to ensure that it is thoroughly cleaned. 2. ** Change paint container ** - A new paint container was installed, and the corresponding clamp was used to fix the container to ensure safety and reliability. ** IV. Replacing the valve and sensor ** 1. ** Replacing the valve ** - First of all, determine which valve needs to be replaced, then use professional equipment to disassemble it, and choose a suitable position for the new valve to install. 2. ** Replacing the sensor ** - Clean the original sensor, then remove it and mark it according to the location where the new sensor is to be installed. For the modification of the reactor involving the key supervision of dangerous chemical processes (such as the modification of the internal heat-conducting oil-injected electric heating reactor without cooling measures): 1. ** For the atmospheric pressure reaction process using heat medium heating ** - The reaction kettle should be equipped with automatic control valve for feed and heat medium, and the reaction temperature can be adjusted by changing the feed flow or heat medium flow. - The reaction kettle shall be equipped with a high reaction temperature alarm and interlocked to cut off the feed or the heat medium. The parallel lock shall be used to open the emergency cooling system (including the cooling medium) and emergency discharge facilities. 2. ** For the pressure reaction process using heat medium heating ** - The reaction kettle should be equipped with an automatic feed or heat medium flow control valve, which can adjust the reaction temperature and pressure by changing the feed flow or heat medium flow. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Zhoushan reaction kettle electric heating
Zhoushan electric heating heat-conducting oil furnace has been applied in the production of oil resin. In industrial production, the reaction kettle electric heating heat-conducting oil furnace had many advantages. For example, its heating system was a closed circulation system, which could quickly heat up and cool down the reaction kettle. It could be customized to a very small volume and was easy to install. It was suitable for medical research occasions. It could realize special control methods such as cascaded control to stabilize the temperature. It could also realize automatic control through remote communication or programming with a PC to provide safety for production. It also played a positive role in reducing the probability of defective products and providing complex temperature control process design solutions. Its power consumption mainly depends on the heating part and the circulating pump, and the power consumption can be reduced through measures such as pipe insulation. In the relevant application scenarios of Zhoushan, the electric heating oil furnace of the reactor could also play a similar role. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Reaction kettle equipment recycling price
The recycling price of the reactor equipment is as follows: - Second-hand stainless steel reactors were priced at 400 - 500 yuan. - The factory's direct selling price for the reaction kettle was 60 - 100 yuan. - The price of second-hand reactors was quoted at 100 - 400 yuan. - The direct selling price of the reaction kettle was 50 - 200 yuan. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>
Sichuan 2000L Enamel Reaction Kettle
Regarding the Sichuan 2000L porcelain reactor, no special information was found. However, the general porcelain reactor was composed of a pot body, a pot cover, a stirring device, a jacket, a support and transmission device, a shaft sealing device, etc. The porcelain reaction surface was coated with a porcelain glaze containing high SiO2 on the inner surface of the metal container of the reaction kettle. After being roasted at a high temperature of about 950 ° C, the porcelain glaze was tightly adhered to the surface of the metal iron body of the reaction kettle, forming a smooth and clean lining layer. Therefore, it had the double advantages of glass-like stability and metal strength. It had excellent corrosion resistance and was widely used in the chemical industry. Food, paint, hot melt glue, silica gel, paint, medicine, reaction, evaporating, synthesis, extraction, concentration, etc. The suitable medium in the kettle is various concentration of mineral acid, organic acid, organic solution and weak base solution. It cannot be used for strong base and any concentration and temperature (temperature greater than or equal to 180 ° C, concentration greater than 30% of phosphorous acid, etc.). In terms of operation and usage, there were corresponding operating specifications and precautions. <a href="/?from=ask_words" style="color:red" target="_blank">Read more exciting novels for free</a>